论文标题
严重的热氧化老化对短玻璃纤维增强PA6/6.6的机械行为和疲劳耐用性的影响
Effect of severe thermo-oxidative aging on the mechanical behavior and fatigue durability of short glass fiber reinforced PA6/6.6
论文作者
论文摘要
这项工作涉及短纤维增强热塑性(SFRP)的疲劳寿命估计,重点是热衰老的共轭作用。在空气中,有两种含有35%(V35)和50%(V50)的重量比在200 {\ textdegree} C时老化了500h,并将其与干燥(DAM)状态的相同材料相比。在注入的板上加工的样品中进行单调和疲劳测试,并沿着注射1(0、45、90 {\ textDegree})沿三个不同方向进行切割,以捕获注射SFRP中经典的皮肤核微结构的各向异性。单调拉伸测试证明了文献中报道的聚酰胺基质的僵硬和覆盖,但取决于基质比和纤维方向的敏锐度。在恒定幅度,频率(10Hz),温度(200 {\ TextDegree} C)和应力比r = 0.1时进行应力控制的疲劳测试。 V35的疲劳曲线比V50材料的衰老影响更大。平均应变演变和SEM观察结果的综合结果证实,疲劳寿命估计的起始方法在老年复合材料中仍然有效。从该数据库中评估了一些疲劳标准,其中包括文献中最近报道的。初步分析了衰老对参与标准的不同疲劳指标参数(FIP)的影响。对于当前的疲劳条件,未经覆盖材料的最佳标准(即基于环状的蠕变能量)仍然是对老年材料的最佳标准。最后,评估了从鉴定未衰老状态下的疲劳标准来预测老年复合材料疲劳寿命的能力。
The work deals with the fatigue lifetime estimation of Short Fiber Reinforced Thermoplastics (SFRP), with a focus on conjugated effects of thermal aging. Two materials containing 35% (V35) and 50% (V50) weight ratio of short glass fibers were aged for 500h at 200{\textdegree}C in air and compared to the same materials in a Dry-As-Molded (DAM) state. Monotonic and fatigue tests were performed in samples machined out of injected plates and cut along three different orientations to the injection one (0, 45, 90{\textdegree}) in order to capture the anisotropy of the skin-core microstructure, classical in injected SFRP. Monotonic tensile tests evidenced the stiffening and embrittlement of the Polyamide matrix reported in the literature, nevertheless with an acuity depending on the matrix ratio and fiber orientation. Stress-controlled fatigue tests were performed at constant amplitude, frequency (10Hz), temperature (200{\textdegree}C) and stress ratio R=0.1. The fatigue curves of V35 are more affected by aging than those of the V50 material. The combined results from the mean strain evolutions and SEM observations confirmed that the initiation approach for fatigue lifetime estimation was still valid in aged composites. Several fatigue criteria, among the most recently reported in the literature, were evaluated from this database. The effect of aging on the cyclic evolution of the different Fatigue Indicator Parameters (FIP) involved in the criteria was analyzed preliminarily. For the present fatigue conditions, the best criteria for unaged materials (i.e cyclic creep energy-based ones) were shown to still be the best for aged materials. Finally, the ability to predict fatigue lifetime for aged composites from the identification of the fatigue criterion in the unaged state was evaluated.